<\/p>\n
Structural formula<\/p>\n
None<\/p>\n<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n
CAS number:<\/b>96-35-5<\/p>\n
MDL number:<\/b>MFCD00004667<\/p>\n
EINECS number:<\/b>202-502-7<\/p>\n
RTECS number:<\/b>None<\/p>\n
BRN number:<\/b>1699571<\/p>\n
PubChem number:<\/b>24859497<\/p>\nPhysical property data<\/h2>\n
1. Properties: colorless liquid. <\/p>\n
2. Density (g\/mL, 25\u2103): 1.167<\/p>\n
3. Relative vapor density (g\/mL, air=1): 3.12<\/p>\n
4. Melting point (\u00baC): Undetermined<\/p>\n
5. Boiling point (\u00baC, normal pressure): 149-151<\/p>\n
6. Boiling point (\u00baC, kPa): Undetermined<\/p>\n
7. Refractive index: 1.417<\/p>\n
8. Flash point (\u00baC): 67<\/p>\n
9. Specific rotation (\u00ba): Undetermined<\/p>\n
10. Autoignition point or ignition temperature (\u00baC): Undetermined<\/p>\n
11. Vapor pressure (mmHg, 52\u00baC): 17<\/p>\n
12. Saturated vapor pressure (kPa, \u00baC) : Undetermined<\/p>\n
13. Heat of combustion (KJ\/mol): Undetermined<\/p>\n
14. Critical temperature (\u00baC): Undetermined<\/p>\n
15. Critical pressure (KPa): Undetermined<\/p>\n
16. Log value of oil-water (octanol\/water) distribution coefficient: Undetermined<\/p>\n
17. Explosion upper limit (%, V\/V): Undetermined Determined<\/p>\n
18. Lower explosion limit (%, V\/V): Undetermined<\/p>\n
19. Solubility: Undetermined<\/p>\n<\/p>\n
\n None\n <\/p>\n
This substance is slightly hazardous to water. <\/p>\n<\/p>\n
1. Molar refractive index: 19.25<\/p>\n
2. Molar volume (cm3<\/sup>\/mol): 79.0<\/p>\n3. Isotonic specific volume (90.2K ): 192.9<\/p>\n4. Surface tension (dyne\/cm): 35.5<\/p>\n5. Polarizability (10-24cm3): 7.63<\/p>\n<\/p>\nCompute chemical data<\/h2>\n1. Reference value for hydrophobic parameter calculation (XlogP): -0.5<\/P><\/p>\n2. Number of hydrogen bond donors: 1<\/p>\n3. Number of hydrogen bond acceptors: 3<\/p>\n p><\/p>\n4. Number of rotatable chemical bonds: 2<\/p>\n5. Number of tautomers: none<\/p>\n6. Topological molecule polar surface area 46.5<\/p>\n7. Number of heavy atoms: 6<\/p>\n8. Surface charge: 0<\/p>\n9. Complexity: 50<\/p>\n10. Number of isotope atoms: 0<\/p>\n11. Determine the number of atomic stereocenters: 0<\/p>\n12. Uncertain number of atomic stereocenters: 0<\/p>\n13. Determine the number of chemical bond stereocenters: 0<\/p>\n14. Number of uncertain chemical bond stereocenters: 0<\/p>\n15. Number of covalent bond units: 1<\/p>\n<\/p>\nProperties and stability<\/h2>\nAvoid contact with oxidizing agents. <\/p>\n<\/p>\nStorage method<\/h2>\n\n Store in a cool, ventilated warehouse. Keep away from fire and heat sources. They should be stored separately from oxidants, and avoid mixed storage.\ufffd\ufffdAdopt explosion-proof lighting and ventilation facilities. It is prohibited to use mechanical equipment and tools that are prone to sparks. The storage area should be equipped with emergency spill treatment equipment and suitable containment materials.\n <\/p>\nSynthesis method<\/h2>\n1. Preparation method: <\/p>\nIn a reaction flask equipped with a stirrer and a reflux condenser, heat 940g (10mol) of chloroacetic acid (2) and 1.33kg of 30% sodium hydroxide solution (10 mol), react in boiling water bath for 1 hour with stirring. Concentrate under reduced pressure, filter out the precipitated sodium chloride in stages, wash the sodium chloride with a small amount of water, repeat this process several times, and filter out a total of 550-600g of sodium chloride. Finally, the water pump is depressurized and the oil bath is heated to 160\u00b0C. Cool to 100\u00b0C and filter to obtain a slurry liquid. Neutralize by heating sodium carbonate, leave overnight, and filter. Steam off the methanol, fractionate under reduced pressure, and collect the fractions at 65~85\u2103\/6.7~8.0kPa. After adjusting the pH, filter and fractionate again to obtain 270g of product (1) with a yield of 30%. [1]<\/sup><\/p>\n<\/p>\nPurpose<\/h2>\nHigh-end cleaning solvent for organic synthesis. <\/p>\n<\/p>\n extended-reading:https:\/\/www.newtopchem.com\/archives\/44947<\/a><\/br>extended-reading:https:\/\/www.newtopchem.com\/archives\/558<\/a><\/br>extended-reading:https:\/\/www.bdmaee.net\/polyurethane-retardation-catalyst-c-225\/<\/a><\/br>extended-reading:https:\/\/www.bdmaee.net\/lupragen-n100-catalyst-basf\/<\/a><\/br>extended-reading:https:\/\/www.newtopchem.com\/archives\/44365<\/a><\/br>extended-reading:https:\/\/www.bdmaee.net\/nt-cat-t16-catalyst-cas10102-43-9-newtopchem\/<\/a><\/br>extended-reading:https:\/\/www.bdmaee.net\/teda-l33-polyurethane-amine-catalyst-tosoh\/<\/a><\/br>extended-reading:https:\/\/www.cyclohexylamine.net\/reactive-amine-catalyst-pt305-dabco-amine-catalyst\/<\/a><\/br>extended-reading:https:\/\/\/\/www.bdmaee.net\/wp-content\/uploads\/2022\/08\/N-Formylmorpholine-CAS4394-85-8-4-formylmorpholine.pdf<\/a><\/br>extended-reading:https:\/\/www.bdmaee.net\/cas-108-01-0\/<\/a><\/p>\n","protected":false,"gt_translate_keys":[{"key":"rendered","format":"html"}]},"excerpt":{"rendered":"Structural formula Business number 02B1 Molecular formu…<\/p>\n","protected":false,"gt_translate_keys":[{"key":"rendered","format":"html"}]},"author":1,"featured_media":48804,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":[],"categories":[6],"tags":[9749],"gt_translate_keys":[{"key":"link","format":"url"}],"_links":{"self":[{"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/posts\/48805"}],"collection":[{"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/comments?post=48805"}],"version-history":[{"count":0,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/posts\/48805\/revisions"}],"wp:featuredmedia":[{"embeddable":true,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/media\/48804"}],"wp:attachment":[{"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/media?parent=48805"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/categories?post=48805"},{"taxonomy":"post_tag","embeddable":true,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/tags?post=48805"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}
3. Isotonic specific volume (90.2K ): 192.9<\/p>\n
4. Surface tension (dyne\/cm): 35.5<\/p>\n
5. Polarizability (10-24cm3): 7.63<\/p>\n<\/p>\n
1. Reference value for hydrophobic parameter calculation (XlogP): -0.5<\/P><\/p>\n
2. Number of hydrogen bond donors: 1<\/p>\n
3. Number of hydrogen bond acceptors: 3<\/p>\n
p><\/p>\n
4. Number of rotatable chemical bonds: 2<\/p>\n
5. Number of tautomers: none<\/p>\n
6. Topological molecule polar surface area 46.5<\/p>\n
7. Number of heavy atoms: 6<\/p>\n
8. Surface charge: 0<\/p>\n
9. Complexity: 50<\/p>\n
10. Number of isotope atoms: 0<\/p>\n
11. Determine the number of atomic stereocenters: 0<\/p>\n
12. Uncertain number of atomic stereocenters: 0<\/p>\n
13. Determine the number of chemical bond stereocenters: 0<\/p>\n
14. Number of uncertain chemical bond stereocenters: 0<\/p>\n
15. Number of covalent bond units: 1<\/p>\n<\/p>\n
Avoid contact with oxidizing agents. <\/p>\n<\/p>\n
\n Store in a cool, ventilated warehouse. Keep away from fire and heat sources. They should be stored separately from oxidants, and avoid mixed storage.\ufffd\ufffdAdopt explosion-proof lighting and ventilation facilities. It is prohibited to use mechanical equipment and tools that are prone to sparks. The storage area should be equipped with emergency spill treatment equipment and suitable containment materials.\n <\/p>\n
1. Preparation method: <\/p>\n
In a reaction flask equipped with a stirrer and a reflux condenser, heat 940g (10mol) of chloroacetic acid (2) and 1.33kg of 30% sodium hydroxide solution (10 mol), react in boiling water bath for 1 hour with stirring. Concentrate under reduced pressure, filter out the precipitated sodium chloride in stages, wash the sodium chloride with a small amount of water, repeat this process several times, and filter out a total of 550-600g of sodium chloride. Finally, the water pump is depressurized and the oil bath is heated to 160\u00b0C. Cool to 100\u00b0C and filter to obtain a slurry liquid. Neutralize by heating sodium carbonate, leave overnight, and filter. Steam off the methanol, fractionate under reduced pressure, and collect the fractions at 65~85\u2103\/6.7~8.0kPa. After adjusting the pH, filter and fractionate again to obtain 270g of product (1) with a yield of 30%. [1]<\/sup><\/p>\n<\/p>\nPurpose<\/h2>\nHigh-end cleaning solvent for organic synthesis. <\/p>\n<\/p>\n extended-reading:https:\/\/www.newtopchem.com\/archives\/44947<\/a><\/br>extended-reading:https:\/\/www.newtopchem.com\/archives\/558<\/a><\/br>extended-reading:https:\/\/www.bdmaee.net\/polyurethane-retardation-catalyst-c-225\/<\/a><\/br>extended-reading:https:\/\/www.bdmaee.net\/lupragen-n100-catalyst-basf\/<\/a><\/br>extended-reading:https:\/\/www.newtopchem.com\/archives\/44365<\/a><\/br>extended-reading:https:\/\/www.bdmaee.net\/nt-cat-t16-catalyst-cas10102-43-9-newtopchem\/<\/a><\/br>extended-reading:https:\/\/www.bdmaee.net\/teda-l33-polyurethane-amine-catalyst-tosoh\/<\/a><\/br>extended-reading:https:\/\/www.cyclohexylamine.net\/reactive-amine-catalyst-pt305-dabco-amine-catalyst\/<\/a><\/br>extended-reading:https:\/\/\/\/www.bdmaee.net\/wp-content\/uploads\/2022\/08\/N-Formylmorpholine-CAS4394-85-8-4-formylmorpholine.pdf<\/a><\/br>extended-reading:https:\/\/www.bdmaee.net\/cas-108-01-0\/<\/a><\/p>\n","protected":false,"gt_translate_keys":[{"key":"rendered","format":"html"}]},"excerpt":{"rendered":"Structural formula Business number 02B1 Molecular formu…<\/p>\n","protected":false,"gt_translate_keys":[{"key":"rendered","format":"html"}]},"author":1,"featured_media":48804,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":[],"categories":[6],"tags":[9749],"gt_translate_keys":[{"key":"link","format":"url"}],"_links":{"self":[{"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/posts\/48805"}],"collection":[{"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/comments?post=48805"}],"version-history":[{"count":0,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/posts\/48805\/revisions"}],"wp:featuredmedia":[{"embeddable":true,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/media\/48804"}],"wp:attachment":[{"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/media?parent=48805"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/categories?post=48805"},{"taxonomy":"post_tag","embeddable":true,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/tags?post=48805"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}
High-end cleaning solvent for organic synthesis. <\/p>\n<\/p>\n
extended-reading:https:\/\/www.newtopchem.com\/archives\/44947<\/a><\/br>extended-reading:https:\/\/www.newtopchem.com\/archives\/558<\/a><\/br>extended-reading:https:\/\/www.bdmaee.net\/polyurethane-retardation-catalyst-c-225\/<\/a><\/br>extended-reading:https:\/\/www.bdmaee.net\/lupragen-n100-catalyst-basf\/<\/a><\/br>extended-reading:https:\/\/www.newtopchem.com\/archives\/44365<\/a><\/br>extended-reading:https:\/\/www.bdmaee.net\/nt-cat-t16-catalyst-cas10102-43-9-newtopchem\/<\/a><\/br>extended-reading:https:\/\/www.bdmaee.net\/teda-l33-polyurethane-amine-catalyst-tosoh\/<\/a><\/br>extended-reading:https:\/\/www.cyclohexylamine.net\/reactive-amine-catalyst-pt305-dabco-amine-catalyst\/<\/a><\/br>extended-reading:https:\/\/\/\/www.bdmaee.net\/wp-content\/uploads\/2022\/08\/N-Formylmorpholine-CAS4394-85-8-4-formylmorpholine.pdf<\/a><\/br>extended-reading:https:\/\/www.bdmaee.net\/cas-108-01-0\/<\/a><\/p>\n","protected":false,"gt_translate_keys":[{"key":"rendered","format":"html"}]},"excerpt":{"rendered":"Structural formula Business number 02B1 Molecular formu…<\/p>\n","protected":false,"gt_translate_keys":[{"key":"rendered","format":"html"}]},"author":1,"featured_media":48804,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":[],"categories":[6],"tags":[9749],"gt_translate_keys":[{"key":"link","format":"url"}],"_links":{"self":[{"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/posts\/48805"}],"collection":[{"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/comments?post=48805"}],"version-history":[{"count":0,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/posts\/48805\/revisions"}],"wp:featuredmedia":[{"embeddable":true,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/media\/48804"}],"wp:attachment":[{"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/media?parent=48805"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/categories?post=48805"},{"taxonomy":"post_tag","embeddable":true,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/tags?post=48805"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}
Structural formula Business number 02B1 Molecular formu…<\/p>\n","protected":false,"gt_translate_keys":[{"key":"rendered","format":"html"}]},"author":1,"featured_media":48804,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":[],"categories":[6],"tags":[9749],"gt_translate_keys":[{"key":"link","format":"url"}],"_links":{"self":[{"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/posts\/48805"}],"collection":[{"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/comments?post=48805"}],"version-history":[{"count":0,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/posts\/48805\/revisions"}],"wp:featuredmedia":[{"embeddable":true,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/media\/48804"}],"wp:attachment":[{"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/media?parent=48805"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/categories?post=48805"},{"taxonomy":"post_tag","embeddable":true,"href":"http:\/\/www.newtopchem.com\/wp-json\/wp\/v2\/tags?post=48805"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}
![\"Methyl](\"http:\/\/www.newtopchem.com\/wp-content\/uploads\/2024\/05\/6731acdd60e5469ea761c8e1b399ea79.gif\")
<\/p>\n<\/p>\n